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chemistry
Posted: 03 Jun 2015, 13:56
by glenpaul
Hi
Does anyone have success when filtering Barium Sulfate? We use Buchner Funnels with the filter paper for barium sulfate from Sc Supply and vacuum pumps on taps but we still don't seem to have success as the sulfate goes through the paper and the solution in the side arm flask is always milky.
Re: chemistry
Posted: 04 Jun 2015, 09:08
by rae
We use Gooch crucibles with the side arm flasks and vacuum pumps and have had great success. The gooch crucible is a sintered glass crucible with a porcelain filter in the bottom. I think the No.4 is what you need. They are expensive but have always worked for us.
Re: chemistry
Posted: 04 Jun 2015, 09:17
by sunray18
Buy Whatman filter papers - No 40 could be the one you need but ask the supplier. They are expensive.
Re: chemistry
Posted: 04 Jun 2015, 10:01
by Mother
I was going to suggest Whatman Grade 42 filters.
Mother
Re: chemistry
Posted: 04 Jun 2015, 10:46
by Loopy
We have good results using Chemistry Contexts 2nd edition prac 3.2 which uses a 0.1% agar solution as a coagulant.
It says " The BaSO4 precipitate is exceedingly fine and is extremely difficult to filter without the uses of agar solution as a coagulating agent. The procedure is valid because the filtrate is clear of any BaSO4 and any agar retained with the BaSO4 residue is of immeasurable mass. If all of the agar was retained, it would add 0.01g to the BaSO4 residue. The sensitivity of the standard laboratory electronic balance is 0.01g"
Hope this helps....
Re: chemistry
Posted: 04 Jun 2015, 11:12
by rae
Loopy is it possible to get a copy of that prac?
Re: chemistry
Posted: 04 Jun 2015, 11:42
by Loopy
I will try. My IT capabilities rate very low!....
Re: chemistry
Posted: 04 Jun 2015, 11:53
by Loopy
Here goes, sorry about the writing on the pages....
Re: chemistry
Posted: 04 Jun 2015, 11:55
by rae
Thanks Loopy it worked a treat!!
Re: chemistry
Posted: 04 Jun 2015, 12:02
by ELIZABETH
Thanks indeed!
Re: chemistry
Posted: 09 Jun 2015, 15:37
by glenpaul
Hi Loopy
Is it possible to have a copy of the "Barium Sulfate /Agar" prac too.
Thanks
Glenpaul
Re: chemistry
Posted: 11 Jun 2015, 09:45
by Loopy
Hi all,
I hope the prac works well for those who try it. Glenpaul, I think the pdf is till available on this page for you to download. Let me know if there are any problems.